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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1589293Erstellt: 25. Oktober 2026

Phenol → 2,4,6-Tris(2-methylbutan-2-yl)phenol

https://huagongshe.com/reaction/1589293

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPhenolHCID 996—
Edukt4-tert-PentylphenolHCID 6643—
Edukt2,4-Di-tert-pentylphenolHCID 8455—
Edukt2-tert-AmylphenolHCID 76769—
Produkt2,4,6-Tris(2-methylbutan-2-yl)phenolHCID 1517385510,8%

Reaktionsschritte

The procedure of Example 1 was repeated except that 1.00 g (10.6 millimoles) of phenol, 11.4 g of the same C5 fraction as used in Example 1, and 1.00 g of Silica-Alumina "IS-28" (produced by Shokubai Kasei Kogyo Co., Ltd.) which had been burned at 500° C. for 10 hours were used. The acid strength of the silica alumina (as determined in the same manner as in Example 1) was as follows: H0 ≤- 8.2. The proportion of the unreacted phenol was 5.0%, and 0.05 g (2.9%) of o-tert-amylphenol, 0.22 g (12.6%) of p-tertamylphenol, 1.73 g (69.6%) of 2,4-di-tert-amylphenol, and 0.01 g (0.3%) of 2,4,6-tri-tert-amylphenol were formed.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04568778
Quelldatensatzuspto-grants-1986_02
ORD IDord-e60bef2d4ba84997af8d0ec51740afcf
Quellennotizuspto-grants-1986_02