HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86740078, compound → HCID 86740079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86740078 | HCID 86740078 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86740079 | HCID 86740079 | 74.6% |
Reaction Steps
To 100 ml of methanol, were added 2.0 g of 4-amidino-2-methoxyphenyl cinnamate methanesulfonate and 0.5 g of a 10% palladium-carbon. Hydrogen was fed to the mixture which was stirred vigorously to facilitate absorption. The reaction mixture was freed from the insolubles by filtration and from the solvent by distillation. The residue was recrystallized from ethanol to obtain 1.5 g of the same 4-amidino-2-methoxyphenyl 3-phenylpropionate methanesulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04570006 |
| Source dataset | uspto-grants-1986_02 |
| ORD ID | ord-cadf4aabff8745be81f619e9e1515fd7 |
| Source note | uspto-grants-1986_02 |