1-Chloro-4-nitrobenzene → HCID 20245794, compound

HRID 1589704Notes

Reaction equation

HRID 1589704 reaction equation
[CH2:1]([O:8][C:9]1[C:10]([CH3:25])=[C:11]2[C:16](=[C:17]([CH3:20])[C:18]=1[CH3:19])[O:15][C:14]([CH2:22][CH2:23][OH:24])([CH3:21])[CH2:13][CH2:12]2)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[C:27]1[CH:32]=[CH:31][C:30]([N+:33]([O-:35])=[O:34])=[CH:29][CH:28]=1>>[CH2:1]([O:8][C:9]1[C:10]([CH3:25])=[C:11]2[C:16](=[C:17]([CH3:20])[C:18]=1[CH3:19])[O:15][C:14]([CH3:21])([CH2:22][CH2:23][O:24][C:27]1[CH:32]=[CH:31][C:30]([N+:33]([O-:35])=[O:34])=[CH:29][CH:28]=1)[CH2:13][CH2:12]2)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 74741-Chloro-4-nitrobenzeneHCID 109698772-(6-Benzyloxy-2,5,7,8-tetramethylchroman-2-yl)ethanol

Product 1

HCID 20245794HCID 20245794, compound

Procedure

2-(6-Benzyloxy-2,5,7,8-tetramethylchroman-2-yl)ethanol (prepared as described in Preparation 39) was reacted with p-chloronitrobenzene and the reaction mixture was treated and purified as described in Preparation 2, to give the title compound.

Workup

  1. additionthe reaction mixture was treated
  2. custompurified
  3. customas described in Preparation 2

Sources & evidence

ORD record
ord-40c84ba35056487dafe2af098be23145
Source dataset
uspto-grants-1986_02
Patent number
US04572912

Reaction notes

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