Ethanol → HCID 19770591, compound

Participants

Reaction Steps

18 ml of ethanol was added to 10.0 g of ethyl 4-decylbenzoate, and then 20 g of 80%-hydrazine hydrate was added thereto, followed by refluxing for 16 hours. After the reaction, the reaction mixture was poured into 200 ml of iced water to precipitate a crystal. The crystal was recovered by filtration and recrystallized from ethanol to obtain 6.93 g of 4-decylbenzohydrazide (Yield: 72.9%).

Provenance & Evidence