HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178479543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Benzonitrile, 4-bromo- | HCID 12162 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178479543 | HCID 178479543 | — |
Reaction Steps
Compound [H], 4-bromobenzoic acid is chlorinated with thionyl chloride to yield compound [I], 4-bromobenzoic acid chloride. Compound [I] is reacted with aqueous ammonia to yield compound [J] 4-bromobenzoic acid amide. Compound [J] is dehydrated with thionyl chloride to yield compound [K], a 4-bromobenzonitrile. Compound [K] is reacted with gaseous hydrogen chloride in anhydrous ethanol to yield compound [L], 4-bromobenzimidate hydrogen chloride. In ethanol, compound [L] is reacted with gaseous ammonia to yield compound [M], 4-bromobenzamidine hydrogen chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05200110 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-f5c30cdf17ff4cfcb922d02fbd340bb0 |
| Source note | uspto-grants-1993_04 |