HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178447883, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178447888 | HCID 178447888 | — |
| Product | HCID 178447883 | HCID 178447883 | 96.2% |
Reaction Steps
In 75 cm3 (1.0 mol) of SOCl2, 128 g (0.52 mol) of 4-(trans-4'-propylcyclohexyl) benzoic acid was refluxed for 3 hours. The excess SOCl2 was distilled off under a reduced pressure and the residue was distilled under reduced pressure (158° C./3.0 mmHg) to yield 133 g (0.50 mol) of 4-(trans-4'-propylcyclohexyl) benzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05200110 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-8eaca0e6aa924d44805999afc6b806fe |
| Source note | uspto-grants-1993_04 |