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HRID1589790

反应详情

EQUATION

反应方程式

HRID 1589790 的结构方程式

REACTANTS

反应物

3
结构：O=[N+]([O-])c1ccc2nc(Cl)c(Cl)nc2c1
HCID689090

2,3-Dichloro-6-nitroquinoxaline

C8H3Cl2N3O2

结构：O=[N+]([O-])c1cc2nc(Cl)c(Cl)nc2cc1[N+](=O)[O-]
HCID3398391

2,3-dichloro-6,7-dinitroquinoxaline

C8H2Cl2N4O4

结构：N#CC(C#N)=C(S[K])S[K]
HCID178511138

未命名化合物

PRODUCTS

生成物

1
结构：N#CC(C#N)=C1Sc2nc3cc([N+](=O)[O-])c([N+](=O)[O-])cc3nc2S1
HCID19770830

未命名化合物

收率 82%

PROCEDURE

实验过程

The process of Example 13 is followed except that the 2,3-dichloro-6-nitroquinoxaline is replaced by 1.25 g of 2,3-dichloro-6,7-dinitroquinoxaline and 1.13 g of the di(potassiomercapto)methylenemalononitrile is used. The recovered material is a dark brown powder weighing 1.26 g with a calculated overall yield of 82 percent and has a melting point greater than 300° C.