Sulfuric Acid → HCID 15005905, compound

HRID 1589855Notes

Reaction equation

HRID 1589855 reaction equation
Br[CH:2](Br)[C:3]1[C:8]2[N:9]=[C:10]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[O:11][C:7]=2[CH:6]=[CH:5][CH:4]=1.S(=O)(=O)(O)[OH:20]>O>[C:12]1([C:10]2[O:11][C:7]3[C:8](=[C:3]([CH:2]=[O:20])[CH:4]=[CH:5][CH:6]=3)[N:9]=2)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 2

HCID 1118Sulfuric AcidHCID 15676494HCID 15676494, compound

Product 1

HCID 15005905HCID 15005905, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

5.5 g (14.9 mmol) of the compound from Example XII were stirred at 100° C. with 30 ml of concentrated sulphuric acid for 1 h, the mixture was poured into water, and the precipitate was filtered off with suction and dried.

Workup

  1. filtrationthe precipitate was filtered off with suction
  2. customdried

Sources & evidence

ORD record
ord-ebfcd45210da4a98959121189c050cfa
Source dataset
uspto-grants-1993_04
Patent number
US05200420

Reaction notes

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