O-Phenylenediamine → 2-(2-Nitroanilino)phenol

HRID 1589860Notes

Reaction equation

HRID 1589860 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[NH:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1N)([O-:3])=[O:2].C1(N)C=CC=CC=1N.FC1C=CC=CC=1[N+]([O-])=[O:34]>>[OH:34][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=1[NH:10][C:5]1[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=1[N+:1]([O-:3])=[O:2]

Participants

4

Reactant 3

HCID 7243O-PhenylenediamineHCID 738951-Fluoro-2-nitrobenzeneHCID 14224812N~1~-(2-Nitrophenyl)benzene-1,2-diamine

Product 1

HCID 142248152-(2-Nitroanilino)phenol

Procedure

N-2-nitrophenyl-o-phenylendiamine, M.p. 95°-98° C. by reaction between o-phenylendiamine and 2-fluoronitrobenzene.

Sources & evidence

ORD record
ord-375cfb127d1b485985225d88ef67b3e9
Source dataset
uspto-grants-1993_04
Patent number
US05200422

Reaction notes

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