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HRID1589938

反应详情

EQUATION

反应方程式

HRID 1589938 的结构方程式

REACTANTS

反应物

3
结构：C1CCC(NC2CCCCC2)CC1
HCID7582

Dicyclohexylamine

C12H23N

结构：O=[N+]([O-])c1cccc([N+](=O)[O-])c1CO
HCID119332

(2,6-Dinitrophenyl)methanol

C7H6N2O5

结构：O=S(=O)(Cl)c1ccc(C(F)(F)F)cc1
HCID2777399

4-(Trifluoromethyl)benzenesulfonyl chloride

C7H4ClF3O2S

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cccc([N+](=O)[O-])c1COS(=O)(=O)c1ccc(C(F)(F)F)cc1
HCID18625054

未命名化合物

收率 38%

PROCEDURE

实验过程

The procedure of Example 11 was employed except that the reagents were 2.00 g of 2,6-dinitrobenzyl alcohol, 2.71 g of 4-(trifluoromethyl)benzenesulfonyl chloride and 2.2 mL of dicylohexylamine. The crude product was recrystallized using carbon tetrachloride/chloroform to give 1.55 g (38% yield) of white crystals.

WORKUP

后处理

  1. customThe crude product was recrystallized