HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → Allyl 4-hydroxy-2-methylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | 4-Hydroxy-o-toluic acid | HCID 68475 | — |
| Product | Allyl 4-hydroxy-2-methylbenzoate | HCID 14852523 | 76% |
Reaction Steps
In a manner analogous to Example 1(a), 5.34 g (32 mmoles) of 4-hydroxy-2-methyl benzoic acid treated at 100° C. for 12 hours with 50 ml of allyl alcohol and 1.5 ml of concentrated sulfuric acid, give 4 g (76% yield) of the expected ester having a melting point of 76°-77° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05200550 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-c3b091232f974d1189aede60949857f5 |
| Source note | uspto-grants-1993_04 |