HCID 14852490, compound → 2-Methylbenzoic acid

HRID 1589968Notes

Reaction equation

HRID 1589968 reaction equation
C12(C3C=C(C=CC=3OC)C(O[C:17]3[CH:28]=[CH:27][C:20]([C:21]([O:23]CC=C)=[O:22])=[C:19]([CH3:29])[CH:18]=3)=O)CC3CC(CC(C3)C1)C2.C12(C3C=C(C=CC=3OC)C(OC3C=CC(C(O)=O)=C(C)C=3)=O)CC3CC(CC(C3)C1)C2>>[CH3:29][C:19]1[CH:18]=[CH:17][CH:28]=[CH:27][C:20]=1[C:21]([OH:23])=[O:22]

Participants

3

Reactant 2

HCID 14852490HCID 14852490, compoundHCID 14852491HCID 14852491, compound

Product 1

HCID 83732-Methylbenzoic acid

Procedure

In a manner analogous to Example 2(c), starting with 1.38 g (3 mmoles) of allyl 4-[3-(1-adamantyl)-4-methoxybenzoyloxy]-2-methylbenzoate, 780 mg of 4-[3-(1-adamantyl)-4-methoxybenzoyloxy]-2-methylbenzoic acid having a melting point of 236°-237° C. are obtained.

Workup

  1. customare obtained

Sources & evidence

ORD record
ord-7f45b090947f4d43a7945b94f2df4af3
Source dataset
uspto-grants-1993_04
Patent number
US05200550

Reaction notes

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