HCID 178459109, compound → HCID 178459099, compound

HRID 1590020Notes

Reaction equation

HRID 1590020 reaction equation
[CH:1]([CH2:3][C@H:4]1[CH2:9][CH2:8][C@H:7]([C:10]2[CH:17]=[CH:16][C:13]([C:14]#[N:15])=[CH:12][CH:11]=2)[CH2:6][CH2:5]1)=O.[CH2:18]([O:21][CH2:22]C[C@H]1CC[C@H](C2C=CC(C#N)=CC=2)CC1)[CH:19]=[CH2:20]>>[CH2:18]([O:21][CH2:22][CH2:1][CH2:3][C@H:4]1[CH2:9][CH2:8][C@H:7]([C:10]2[CH:17]=[CH:16][C:13]([C:14]#[N:15])=[CH:12][CH:11]=2)[CH2:6][CH2:5]1)[CH:19]=[CH2:20]

Participants

3

Reactant 2

HCID 178459109HCID 178459109, compoundHCID 178509798HCID 178509798, compound

Product 1

HCID 178459099HCID 178459099, compound

Procedure

The compound (iii) of Example 7 was subjected to the procedures of (ii), (iii), (iv) and (v) of Example 7 in this order to obtain the captioned compound. M.P.: 12.0° C.,N-I point: 5.9° C.

Workup

  1. customto obtain the captioned compound
  2. custom5.9° C.

Sources & evidence

ORD record
ord-6c2dbf09647a4954830a25f8abfcc532
Source dataset
uspto-grants-1993_04
Patent number
US05202055

Reaction notes

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