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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1590075Generated: November 4, 2026

Diazomethane → HCID 19769486, compound

https://huagongshe.com/reaction/1590075

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiazomethaneHCID 9550—
ReactantHCID 10470291HCID 10470291—
SolventDiethyl EtherHCID 3283—
ProductHCID 19769486HCID 19769486—

Reaction Steps

A solution of diazomethane in diethyl ether was added to a solution of (-)-2-(3-benzyloxy-5-fluorophenyl)-2-hydroxybutyric acid (2.24 g) in diethyl ether (35 ml) until the reaction mixture retained a yellow colouration. The mixture was evaporated to give optically active methyl 2-(3-benzyloxy-5-fluorophenyl)-2-hydroxybutyrate (2.27 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05202326
Source datasetuspto-grants-1993_04
ORD IDord-35ca64b0435f4737a0e5512fca22769e
Source noteuspto-grants-1993_04