HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19100960, compound → HCID 19100975, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19100960 | HCID 19100960 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19100975 | HCID 19100975 | — |
Reaction Steps
11 g (43.7 mmol, 93%) of 2-benzyl-5-fluoro-7-methyl-2,7-diazabicyclo[3.3.0]octane in 100 ml of ethanol are hydrogenated on 2 g of palladium/active carbon (10% Pd) at 100° C. and 100 bar. The catalyst is filtered off with suction, the filtrate is concentrated, and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05202337 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-50984df1444c462886c6a6fde073ac34 |
| Source note | uspto-grants-1993_04 |