HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86746703, compound → HCID 86746702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86746703 | HCID 86746703 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86746702 | HCID 86746702 | 93.4% |
Reaction Steps
To a suspension of (E)-2-benzylidene-3-(trans-decahydro- 2-isoquinolylcarbonyl)propionic acid (200 mg) in ethanol (2 ml) was added 10% Pd-C (20 mg) and the mixture was hydrogenated at room temperature and atmospheric pressure for 16 hours. After the catalyst was filtered off, the solvent was evaporated under reduced pressure to give 188 mg of 2-benzyl-3-(trans-decahydro-2-isoquinolylcarbonyl)propionic acid as a colorless viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05202335 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-3b01905dbd6d455d84b610ae8a173b80 |
| Source note | uspto-grants-1993_04 |