Thioglycerol → 2-[3-(2,3-Dihydroxypropylthio)propyl]-6-methylphenol

HRID 1590278Notes

Reaction equation

[CH2:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[C:5]=1[OH:11])[CH:2]=[CH2:3].[SH:12][CH2:13][CH:14]([OH:17])[CH2:15][OH:16]>>[OH:17][CH:14]([CH2:15][OH:16])[CH2:13][S:12][CH2:3][CH2:2][CH2:1][C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[C:5]=1[OH:11]

Participants

Reactant 2

HCID 7291Thioglycerol

HCID 768832-Allyl-6-methylphenol

Product 1

HCID 197701042-[3-(2,3-Dihydroxypropylthio)propyl]-6-methylphenol

Procedure

In the same manner as in Synthetic example 1, 2-allyl-6-methylphenol and 3-mercapto-1,2-propanediol were reacted to obtain 2-[3-(2,3-dihydroxypropylthio)propyl]-6-methylphenol.

Sources & evidence

ORD record: ord-87ee157ba1f94aeeaeb08753b2f9116f
Source dataset: uspto-grants-1993_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05202409

Reaction notes

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