HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → 1-[2-Oxo-2-(2-pyridyl)ethyl]pyridinium Iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | 2-Acetylpyridine | HCID 14286 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 1-[2-Oxo-2-(2-pyridyl)ethyl]pyridinium Iodide | HCID 213499 | — |
Reaction Steps
2-Acetylpyridine (1.21 g, 10.0 mmol) and iodine (2.54 g, 10.0 mmol) were heated to reflux in pyridine (12 ml) for 1 hour. The solution was cooled, and the dark precipitate was filtered and washed with pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05202423 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-c2c806ffd31d49a5b3416506805b435c |
| Source note | uspto-grants-1993_04 |