HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 3-(4-Bromophenyl)prop-2-enyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3-(4-Bromo-phenyl)-prop-2-en-1-ol | HCID 53396371 | — |
| Product | 3-(4-Bromophenyl)prop-2-enyl acetate | HCID 54413835 | 88.2% |
Reaction Steps
3-(4-Bromophenyl)prop-2-en1-ol (2.13 g) (see example 1) was reacted with acetic anhydride (1.2 g) in the usual manner to give 3-(4-bromophenyl)prop-2-enyl acetate (2.25 g) NMR 1H: 7.35(2H,d), 7.08(2H,d), 6.52(1H,d), 6.10(1H,dt), 4.65(2H,d), 2.1(3H,s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05202356 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-0d8faeb0dc194fb2adc8eee6bf8a2342 |
| Source note | uspto-grants-1993_04 |