HCID 53911448, compound → HCID 18651194, compound

Participants

Reaction Steps

The above alcohol (2 g) was treated with diethyl zinc (35 ml) and dioodomethyl 15.52 ml) in hexane in the usual manner to give (±)-[Trans-2-(3,4-dibromophenyl)cyclopropyl]methanol (1.3 g). NMR 1H: 7.40(1H,d), 7.30(1H,d), 6.76(1H,dd), 3.53(2H,d), 2.30(1H,s), 1.68(1H,m), 1.33(1H,m), 0.87(2H,m).

Provenance & Evidence