Dimethyl Sulfoxide → HCID 19769964, compound

Participants

Reaction Steps

The above alcohol (3.18 g) was oxidised using the conditions of Swern oxalyl chloride, 0.96 ml, dimethyl sulphoxide, 1.56 ml; triethylamine, 6.9 ml) in dichloromethane to give 4-(2,2-dibromoethenyl)benzaldehyde (2.04 g). NMR 1H 10.94 (1H,s), 7.86(2H,d), 7.61(2H,d), 7.45(1H,s).

Provenance & Evidence