Sulfuric Acid → HCID 15143345, compound

HRID 1590431Notes

Reaction equation

HRID 1590431 reaction equation
S(=O)(=O)(O)O.[CH3:6][O:7][C:8]1[CH:21]=[CH:20][C:11]([C:12]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:13])=[CH:10][CH:9]=1.C(C1C(O)=CC(C(C)(C)C)=C(C)C=1)(C)(C)C.[CH2:38]([NH:40][C:41](=[O:44])[CH:42]=[CH2:43])O>>[C:41]([NH:40][CH2:38][C:9]1[CH:10]=[C:11]([CH:20]=[CH:21][C:8]=1[O:7][CH3:6])[C:12]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[O:13])(=[O:44])[CH:42]=[CH2:43]

Participants

5

Reactant 4

HCID 1118Sulfuric AcidHCID 13543N-MethylolacrylamideHCID 691464-MethoxybenzophenoneHCID 139813742,5-Di-tert-butyl-4-methylphenol

Product 1

HCID 15143345HCID 15143345, compound

Procedure

A mixture of 1000 g of sulfuric acid, 175.6 g (0.825 mole) of 4-methoxybenzophenone, 0.5 g of 2,5-di-tert-butyl-p-cresol and 86 g (0.851 mole) of N-methylolacrylamide was reacted for 5 hours at 25° C. and then hydrolyzed on ice.

Workup

  1. customwas reacted for 5 hours at 25° C.

Sources & evidence

ORD record
ord-10b78988cf244f40bae38890352ead7d
Source dataset
uspto-grants-1993_04
Patent number
US05202483

Reaction notes

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