Ethylene → tert-Amylbenzene

HRID 1590446Notes

Reaction equation

HRID 1590446 reaction equation
[C:1]1([CH:7]([CH3:9])[CH3:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:10]=[CH2:11]>>[C:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)([CH2:10][CH3:11])([CH3:9])[CH3:8]

Participants

3

Reactant 2

HCID 6325EthyleneHCID 7406Cumene

Product 1

HCID 16295tert-Amylbenzene

Conditions

Temperature
40 °C

Procedure

In a 600 ml autoclave equipped with a magnetic stirrer, Solid Base A-1 (0.63 g) and cumene (240 g) were charged under nitrogen, heated to 40° C. while stirring at 1,000 rpm and then reacted at the same temperature for 3 hours while supplying ethylene gas under pressure of 10 kg/cm2G. to produce tert.-amylbenzene (hereinafter referred to as "TAB").

Workup

  1. customIn a 600 ml autoclave equipped with a magnetic stirrer
  2. customreacted at the same temperature for 3 hours

Sources & evidence

ORD record
ord-a1d87fce04f340dfa39e9064350a5e7a
Source dataset
uspto-grants-1993_04
Patent number
US05202515

Reaction notes

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