HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 135508003, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-Amino-p-cresol | HCID 17820 | — |
| Reactant | Sodium 3-nitrobenzenesulfonate | HCID 31389 | — |
| Solvent | Glycerol | HCID 753 | — |
| Product | HCID 135508003 | HCID 135508003 | 5.8% |
Reaction Steps
Following the same procedure as in Example 23-(a), reaction and treatment were carried out using 3.9 g of 3-amino-4-methylphenol, 7 ml of glycerol, 8.7 g of sodium m-nitrobezene sulfonate and 29 ml of a 80% aqueous sulfuric acid solution in order to obtain 290 mg of 5-hydroxy-8 -methylquinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05204348 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-e3eb1f5b7b21486386e22fa4cb3ac636 |
| Source note | uspto-grants-1993_04 |