HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → L-Proline, 1-(1-oxohexyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 54249075 | HCID 54249075 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | L-Proline, 1-(1-oxohexyl)- | HCID 10751088 | 97.8% |
Reaction Steps
10% Pd-C (3.00 g) was added to a 1% water-containing methanol solution (200 ml) of N-hexanoyl-L-proline benzyl ester (25.61 g), and the mixture was stirred under a hydrogen atmosphere at room temperature for 1.5 hours. After the catalyst was filtered off, the filtrate was concentrated to obtain 17.61 g of N-hexanoyl-L-proline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05204462 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-9021ed3d5eaf4d45a77ef42ddc440104 |
| Source note | uspto-grants-1993_04 |