Di-tert-butyl peroxide → HCID 54457070, compound

Participants

Reaction Steps

A solution of 34.2 g of di-(1-oxyl-2,2,6,6-tetramethylpiperidin-4-yl) isophthalate and 54 ml of di-tert-butyl peroxide in 250 ml of cyclohexane is heated for 22 hours in a nitrogen atmosphere in a Fisher-Porter bottle (bath temperature of 140° C.). Solvent is evaporated under reduced pressure. The product is recrystallized from pentane to give a white solid, mp 140°-42° C.

Provenance & Evidence