Butylamine → HCID 19768373, compound

HRID 1590939Notes

Reaction equation

HRID 1590939 reaction equation
[CH3:1][CH:2]([O:9][N:10]1[C:15]([CH3:17])([CH3:16])[CH2:14][C:13](=O)[CH2:12][C:11]1([CH3:20])[CH3:19])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH2:21]([NH2:25])[CH2:22][CH2:23][CH3:24]>>[CH3:1][CH:2]([O:9][N:10]1[C:15]([CH3:17])([CH3:16])[CH2:14][CH:13]([NH:25][CH2:21][CH2:22][CH2:23][CH3:24])[CH2:12][C:11]1([CH3:20])[CH3:19])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 8007ButylamineHCID 179683592,2,6,6-Tetramethyl-1-(1-phenylethoxy)piperidin-4-one

Product 1

HCID 19768373HCID 19768373, compound

Procedure

The title compound, a colorless oil, is prepared from 1-alpha-methylbenzyloxy-2,2,6,6-tetramethylpiperidine-4-one and butylamine according to the procedure given in Example 35 except that acetonitrile is substituted for tetrahydrofuran and the molecular sieves are omitted.

Sources & evidence

ORD record
ord-5009ad97a8a44b679816fe5e91cc4e19
Source dataset
uspto-grants-1993_04
Patent number
US05204473

Reaction notes

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