HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boc-Thr(Bzl)-Pro-OH → Boc-Thr(Bzl)-Pro-Gln-Thr(Bzl)-Asp(OBzl)-Val-Gly-Ala-Gly-Thr(Bzl)-Pro-NH2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boc-Thr(Bzl)-Pro-OH | HCID 13091018 | — |
| Reactant | Boc-Gln-Thr(Bzl)-Asp(OBzl)-Val-Gly-Ala-Gly-Thr(Bzl)-Pro-NH2 | HCID 15928431 | — |
| Product | Boc-Thr(Bzl)-Pro-Gln-Thr(Bzl)-Asp(OBzl)-Val-Gly-Ala-Gly-Thr(Bzl)-Pro-NH2 | HCID 131717874 | 85.4% |
Reaction Steps
By using 3.08 g of Boc-Gln-Thr(Bzl)-Asp(OBzl)-Val-Gly-Ala-Gly-Thr(Bzl)-Pro-NH2 and 1.52 g of Boc-Thr(Bzl)-Pro-OH, and the same procedure as in Reference Example 15 was repeated to obtain 3.21 g (yield: 85.4%) of the above-mentioned objective product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05204326 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-fdbe1c3d08364f06bcadae005bb877fe |
| Source note | uspto-grants-1993_04 |