Formic Acid → HCID 19766763, compound

Participants

Reaction Steps

6.8 parts of N,N-dimethyl-N'-(4-chloro-3-cyano-5-methylthien-2-yl)-formamidine, 30 parts of formic acid and 30 parts of water are heated at the boil for 1 hour, and the precipitated product is filtered off under suction when the mixture is cooled, and washed with water and dried. 5.6 parts (93% of theory) of N-(4-chloro-3-cyano-5-methylthien-2-yl)-formamide are obtained.

Provenance & Evidence