Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1591466Generated: October 25, 2026

(S)-3-Amino-4,5-dihydro-1H-benzo[b]azepin-2(3H)-one → HCID 18651462, compound

https://huagongshe.com/reaction/1591466

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(S)-3-Amino-4,5-dihydro-1H-benzo[b]azepin-2(3H)-oneHCID 10241317—
Reactant3-(((Benzyloxy)carbonyl)amino)-3-methylbutanoic acidHCID 14551007—
ProductHCID 18651462HCID 18651462—

Reaction Steps

Prepared from 3(S)-amino-2,3,4,5-tetrahydro-1H-1-benzazepin-2-one (Example 1, Step B) and 3-benzyloxycarbonylamino-3-methylbutanoic acid (Example 1, Step E) by the procedure described in Example 1, Step F. FAB-MS: calculated for C23H27N3O4 409; found 410 (M+H,100%). [a]D =- 160° (c=1,CHCl3).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05206235
Source datasetuspto-grants-1993_04
ORD IDord-a83d346f1224478788849bb68f8a6592
Source noteuspto-grants-1993_04