HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3328476, compound → 4-Methyl[1,1'-biphenyl]-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3328476 | HCID 3328476 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Methyl[1,1'-biphenyl]-2-amine | HCID 12559457 | 96% |
Reaction Steps
A solution of 2.4 g of 3-nitro-4-phenyltoluene in 25 mL of methanol was hydrogenated at room temperature and 40 psi over 0.30 g of 5% Pd/C catalyst. The solution was filtered and the filtrate concentrated to give 1.98 g of product. EI-MS: calculated for C13H13N: 183; found 183.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05206235 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-fe42613fd8bf47b5bb03cd9ff3565a3b |
| Source note | uspto-grants-1993_04 |