Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Isoprene butadiene | HCID 168288 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | HCID 86593707 | HCID 86593707 | — |
Reaction Steps
Nishikawa, et al., U.S. Pat. No. 5,436,295, Jul. 25, 1995 describes the reparation of block copolymer using a pressure-proof vessel equipped with a stirrer was charged with 3,000 g of cyclohexane, 50 g of sufficiently dewatered styrene and 0.01 mole of lithium sec-butyl followed by polymerization at 60. degree. C. for 60 minutes, addition of 200 g of a 50/50 by weight mixture of isoprene/butadiene followed by polymerization at 60. degree. C. for 60 minutes and addition of 50 g of styrene followed by polymerization for 60 minutes, to obtain a styrene-isoprene/1,3-butadiene-styrene block copolymer. Hydrogenation was conducted in the same manner as above to obtain a block copolymer having a hydrogenation ratio of 98%. This was named SEEPS-1. The block copolymer's olefinic elastomer block having a glass transition point of not higher than −20. degree. C. and a heat of fusion of crystal of not more than 8 cal/g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07290367B2 |
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| Source dataset | uspto-grants-2007_11 |
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| ORD ID | ord-7907a72c36044a6781ccae5f8e881552 |
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| Source note | uspto-grants-2007_11 |
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