HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-ethoxybenzoic acid → 2,4-Dichloro-6-(5-chloro-2-ethoxy-phenyl)-[1,3,5]triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-ethoxybenzoic acid | HCID 5098570 | — |
| Reactant | 2,4-Dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine | HCID 85827032 | — |
| Product | 2,4-Dichloro-6-(5-chloro-2-ethoxy-phenyl)-[1,3,5]triazine | HCID 85827033 | 31% |
Reaction Steps
Using the method described for the synthesis of 2,4-dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine, 5-chloro-2-ethoxybenzoic acid afforded 2,4-dichloro-6-(5-chloro-2-ethoxy-phenyl)-[1,3,5]triazine (9.5 g, 31% yield). 1H NMR (DMSO-d6) 7.62-7.86 (m, 2H), 7.20-7.31 (m, 1H), 4.20 (m, 2H), 1.37 (m, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07291616B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-723bc7eb56034ae48bc4005a8c33e0ad |
| Source note | uspto-grants-2007_11 |