Propanal → HCID 67214298, compound

HRID 1591793Notes

Reaction equation

HRID 1591793 reaction equation
[ClH:1].[CH:2]1[C:15]2[NH:14][C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[S:7][C:6]=2[CH:5]=[CH:4][C:3]=1[C:16]1[N:17]=[C:18]([CH2:21][NH2:22])[S:19][CH:20]=1.[CH:23](=O)[CH2:24][CH2:25][CH2:26][CH3:27].C(=O)CC>>[ClH:1].[CH:2]1[C:15]2[NH:14][C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[S:7][C:6]=2[CH:5]=[CH:4][C:3]=1[C:16]1[N:17]=[C:18]([CH2:21][NH:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])[S:19][CH:20]=1

Participants

4

Reactant 3

HCID 527PropanalHCID 8063PentanalHCID 67213853HCID 67213853, compound

Product 1

HCID 67214298HCID 67214298, compoundYield 38%

Procedure

The experimental protocol used is the same as that described for Stage 399.1 of Example 399, with the compound of Example 362 and valeraldehyde replacing intermediate 355.2 and propionaldehyde respectively. A dark-coloured solid is obtained with a yield of 38%. MH+=382.2.

Workup

  1. customA dark-coloured solid is obtained with a yield of 38%

Sources & evidence

ORD record
ord-7166b4dc6a234422b05992b37bf8cab1
Source dataset
uspto-grants-2007_11
Patent number
US07291641B2

Reaction notes

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