HCID 10499960, compound → HCID 69273945, compound

Participants

Reaction Steps

Further elution gave as a second fraction 0.1 g (13%) of white solid which was characterized to be 3β-(4-Chlorophenyl)-2α-(5-phenyl-1,3,4-oxadiazol-2-yl)-tropane: 1H NMR (CDCl3) 1.76 (m, 3H), 2.06 (s, 3H), 2.45 (s, 3H), 3.36 (m, 2H), 3.51 (m, 1H), 3.65 (m, 1H), 7.21 (m, 4H), 7.47 (m, 3H) 7.91 (m, 2H); mp 170-171° C.; Anal calcd. for C22H22CIN3O; C, 69.55; H, 5.84; N, 11.06; Cl, 9.33. Found: C, 69.49; H, 5.85; N, 11.01; Cl, 9.41; [α]D+33.060 (c, 0.18; CHCl3).

Provenance & Evidence