HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Bromomethyl)benzoic acid → 4-Bromomethyl-benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Bromomethyl)benzoic acid | HCID 22599 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 4-Bromomethyl-benzoyl chloride | HCID 5068289 | — |
Reaction Steps
A solution of 4-bromomethyl-benzoic acid (8.6 g, 0.04 mol) in 7.23 mL SOCl2 (0.1 mol) is heated to reflux for 5 h. SOCl2 is removed, and the residue is recrystalized from hexane to afford 4-bromomethyl-benzoyl chloride as a white crystalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07291635B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-4a79c20662c046759474bed69bbd1d1f |
| Source note | uspto-grants-2007_11 |