Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Acetylpyridine → [3-(1-Pyridin-2-yl-ethylamino)-propyl]-carbamic acid tert-butyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Acetylpyridine | HCID 14286 | — |
| 반응물 | tert-Butyl (3-aminopropyl)carbamate | HCID 2735700 | — |
| 반응물 | Sodium triacetoxyborohydride | HCID 5049666 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | [3-(1-Pyridin-2-yl-ethylamino)-propyl]-carbamic acid tert-butyl ester | HCID 67272175 | — |
반응 단계
Using General Procedure B: Reaction of (3-Amino-propyl)-carbamic acid tert-butyl ester and 2-acetylpyridine with NaBH(OAc)3 in CH2Cl2 gave [3-(1-pyridin-2-yl-ethylamino)-propyl]-carbamic acid tert-butyl ester as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07291631B2 |
| 출처 데이터셋 | uspto-grants-2007_11 |
| ORD ID | ord-674b6709597a455ab445f81ecb162319 |
| 출처 메모 | uspto-grants-2007_11 |