HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-4-nitro-1-phenoxybenzene → 3-Methyl-4-phenoxyaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-4-nitro-1-phenoxybenzene | HCID 18616691 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Methyl-4-phenoxyaniline | HCID 15550488 | — |
Reaction Steps
2-Methyl-4-nitro-1-phenoxybenzene and 10% Pd/C (3.35 g) were dissolved in 200 mL EtOH and stirred under 1 atmosphere of H2 overnight. The reaction mixture was filtered through Celite with the aid of 50 mL EtOH and concentrated to provide 3-methyl-4-phenoxybenzenamine as an oil, which was used in Step C without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294616B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-e9ee4c09cd5b4058a2ce01362df76e76 |
| Source note | uspto-grants-2007_11 |