Sodium Methoxide → HCID 68441022, compound

Participants

Reaction Steps

To a solution of 4-[(4-methoxyphenyl)methyl]-5-methyl-1-phenyl-3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)-1H-pyrazole(0.38 g) in methanol (5 mL) was added sodium methoxide (28% methanol solution, 0.12 mL), and the mixture was stirred at room temperature for 1 hour. The reaction mixture was concentrated under reduced pressure, and the residue was purified by column chromatography on silica gel (eluent: dichloromethane/methanol=10/1) to give the title compound (0.32 g).

Provenance & Evidence