HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiazolidinedione → 5-(3'-Methylaminobiphenyl-4-ylmethylene)thiazolidine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiazolidinedione | HCID 5437 | — |
| Reactant | 3'-Methylaminobiphenyl-4-carbaldehyde | HCID 1394524 | — |
| Product | 5-(3'-Methylaminobiphenyl-4-ylmethylene)thiazolidine-2,4-dione | HCID 86598941 | 91.7% |
Reaction Steps
In a manner similar to Example 1(d), by reacting 2.9 g (13.7 mmol) of 3′-methylaminobiphenyl-4-carbaldehyde with 1.6 g (13.7 mmol) of 2,4-thiazolidinedione, 3.9 g (91%) of the expected product are obtained after trituration in dichloromethane and ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294639B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-d27f7329995142b2b682b2670ee2ca5b |
| Source note | uspto-grants-2007_11 |