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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1593016Generated: November 2, 2026

Triacetoxyperiodinane → HCID 86603571, compound

https://huagongshe.com/reaction/1593016

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriacetoxyperiodinaneHCID 159087—
Reactant(γS)-4-(Methylsulfonyl)-γ-phenylbenzenepropanolHCID 69264553—
SolventDichloromethaneHCID 6344—
ProductHCID 86603571HCID 86603571—

Reaction Steps

To a solution of (S)-3-phenyl-3-(4-methanesulfonylphenyl)propan-1-ol (244 mg, 0.84 mmol) in DCM (5 mL) was added Dess-Martin periodinane (392 mg, 0.92 mmol) and the resulting mixture was stirred at room temperature for 1.5 h. The mixture was washed with 2M aqueous sodium hydroxide (2×10 mL), dried and evaporated to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07294636B2
Source datasetuspto-grants-2007_11
ORD IDord-ae52171f0fbc435fa9f81d6f147975ad
Source noteuspto-grants-2007_11