HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triacetoxyperiodinane → HCID 86603571, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triacetoxyperiodinane | HCID 159087 | — |
| Reactant | (γS)-4-(Methylsulfonyl)-γ-phenylbenzenepropanol | HCID 69264553 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86603571 | HCID 86603571 | — |
Reaction Steps
To a solution of (S)-3-phenyl-3-(4-methanesulfonylphenyl)propan-1-ol (244 mg, 0.84 mmol) in DCM (5 mL) was added Dess-Martin periodinane (392 mg, 0.92 mmol) and the resulting mixture was stirred at room temperature for 1.5 h. The mixture was washed with 2M aqueous sodium hydroxide (2×10 mL), dried and evaporated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294636B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-ae52171f0fbc435fa9f81d6f147975ad |
| Source note | uspto-grants-2007_11 |