HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 21901931, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 21902072 | HCID 21902072 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21901931 | HCID 21901931 | — |
Reaction Steps
2-[3-(Benzo[1,3]dioxol-5-yloxymethyl)-piperidin-1-yl]-1-[1-(2-methoxy-phenyl)-cyclobutyl]-ethanol (232) was prepared according to the procedures outlined in Example 138, using sodium borohydride (17 mg, 0.453 mmol), and 2-[3-(benzo[1,3]dioxol-5-yloxymethyl)-piperidin-1-yl]-1-[1-(2-methoxy-phenyl)-cyclobutyl]-ethanone (100 mg, 0.227 mmol) in MeOH (1.6 mL); MS+ (440).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294637B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-8474037d650d400ea8b473e2e9609bf4 |
| Source note | uspto-grants-2007_11 |