HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl acetoacetate → HCID 58998981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl acetoacetate | HCID 7757 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 2-Bromo-2',5'-dimethoxyacetophenone | HCID 70997 | — |
| Reactant | 2-(2-Chlorophenyl)ethylamine | HCID 83117 | — |
| Product | HCID 58998981 | HCID 58998981 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 68, using 3-oxo-butyric acid methyl ester as compound of formula R, 2-bromo-1-(2,5-dimethoxy-phenyl)-ethanone as compound of formula S, 2-chloro-phenethylamine as R3—(CH2)m—NH2 and cyclohexylamine as R1R2NH, MS (ISP) 481.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294644B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-178218244ea74971962be24dcb710f73 |
| Source note | uspto-grants-2007_11 |