HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2-Carbamoylmethoxy-4-aminosulfonylphenoxyacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3,4-Bis(carbamoylmethoxy)benzenesulfonyl chloride | HCID 18541237 | — |
| Product | 2-Carbamoylmethoxy-4-aminosulfonylphenoxyacetamide | HCID 58999238 | — |
Reaction Steps
2-Carbamoylmethoxy-4-chlorosulfonylphenoxyacetamide (Intermediate A65, 12.9 g, 0.040 mol) was dissolved in methanolic ammonia and stirred for 16 hr. The solvent was removed at aspirator pressure, and the residue was crystallized in water. The resulting solid was washed with hot water and several additional portions of water. The product, title compound weighed 8.6 g (71%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294716B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-8ab1b7edce2848b2b518371e4d8e97be |
| Source note | uspto-grants-2007_11 |