Vinyltrichlorosilane → HCID 14894580, compound

Participants

Reaction Steps

In a 250 ml three-neck flask, 50 ml of hexamethyldisilazane (38.7 g, 0.24 mol) are admixed with 70 ml of vinyltrichlorosilane (88.9 g, 0.55 mol) and stirred overnight at room temperature. The mixture is fractionated under reduced pressure. After trimethylchlorosilane and excess vinyltrichlorosilane have been distilled off, (1,1-dichloro-1-vinyl)trimethyldisilazane goes over as a clear, colorless liquid. The boiling point is 40° C. at 11 mbar, and the yield is 80%.

Provenance & Evidence