HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[2-(Methylsulfanyl)pyrimidin-5-yl]ethan-1-one → 5-[(E)-3-(2-Methylsulfanylpyrimidin-5-yl)-3-oxopropenyl]indan-1-one O-methyloxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[2-(Methylsulfanyl)pyrimidin-5-yl]ethan-1-one | HCID 12792809 | — |
| Reactant | 1H-Indene-5-carboxaldehyde, 2,3-dihydro-1-(methoxyimino)- | HCID 73012344 | — |
| Product | 5-[(E)-3-(2-Methylsulfanylpyrimidin-5-yl)-3-oxopropenyl]indan-1-one O-methyloxime | HCID 86595414 | 28% |
Reaction Steps
The title compound (2.6 g, 28%) was prepared from the product of Step 1 and the product of Example 1 Step 2 using the method of Example 2 Step 1; MS(ES+) m/e 340 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07297694B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-8f135b757e6549fda0596c8a79e66839 |
| Source note | uspto-grants-2007_11 |