HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinecarboxaldehyde → 2-(1-Methoxyiminoindan-5-yl)-4-(2-methylsulfanylpyrimidin-5-yl)-1-pyridin-4-ylbutane-1,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | 5-[(E)-3-(2-Methylsulfanylpyrimidin-5-yl)-3-oxopropenyl]indan-1-one O-methyloxime | HCID 86595414 | — |
| Product | 2-(1-Methoxyiminoindan-5-yl)-4-(2-methylsulfanylpyrimidin-5-yl)-1-pyridin-4-ylbutane-1,4-dione | HCID 86595415 | 74% |
Reaction Steps
The title compound (2.9 g, 74%) was prepared from the product of Step 2 and 4-pyridinecarboxaldehyde using the method of Example 1 Step 4; MS(ES+) m/e 447 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07297694B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-0a5a12fb68a54214a6d8eb72107b4236 |
| Source note | uspto-grants-2007_11 |