4'-Methoxyacetophenone → HCID 86595416, compound

HRID 1593433Notes

Reaction equation

HRID 1593433 reaction equation
[CH3:1][O:2][N:3]=[C:4]1[C:12]2[C:7](=[CH:8][C:9]([CH:13]=O)=[CH:10][CH:11]=2)[CH2:6][CH2:5]1.[CH3:15][O:16][C:17]1[CH:22]=[CH:21][C:20]([C:23](=[O:25])[CH3:24])=[CH:19][CH:18]=1>>[CH3:1][O:2][N:3]=[C:4]1[C:12]2[C:7](=[CH:8][C:9](/[CH:13]=[CH:24]/[C:23]([C:20]3[CH:21]=[CH:22][C:17]([O:16][CH3:15])=[CH:18][CH:19]=3)=[O:25])=[CH:10][CH:11]=2)[CH2:6][CH2:5]1

Participants

3

Reactant 2

HCID 74764'-MethoxyacetophenoneHCID 730123441H-Indene-5-carboxaldehyde, 2,3-dihydro-1-(methoxyimino)-

Product 1

HCID 86595416HCID 86595416, compoundYield 91%

Procedure

The title compound (7.75 g, 91%) was prepared from the product of Example 1 Step 2 and 1-(4-methoxy-phenyl)ethanone using the method of Example 2 Step 1; MS(ES+) m/e 322 [M+H]+.

Sources & evidence

ORD record
ord-d9598dc1d99f43998854cfde451a0a84
Source dataset
uspto-grants-2007_11
Patent number
US07297694B2

Reaction notes

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