HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isovaleryl chloride → N-[4-(5-Cyano-1-methyl-1H-pyrrol-2-yl)phenyl]-3-methylbutanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isovaleryl chloride | HCID 66054 | — |
| Reactant | 5-(4-aminophenyl)-1-methyl-1H-pyrrole-2-carbonitrile | HCID 16050430 | — |
| Product | N-[4-(5-Cyano-1-methyl-1H-pyrrol-2-yl)phenyl]-3-methylbutanamide | HCID 16037460 | — |
Reaction Steps
The title compound was prepared according to the general procedure for acylation of 5-(4-aminophenyl)-1-methyl-1H-pyrrole-2-carbonitrile using 3-methyl-butyryl chloride (67 μL, 0.55 mmol) to provide N-[4-(5-cyano-1-methyl-1H-pyrrol-2-yl)phenyl]-3-methyl butanamide (0.042 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07297713B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-85b5854606e649e48862b133ed7e8a84 |
| Source note | uspto-grants-2007_11 |