HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 58999582, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178516359 | HCID 178516359 | — |
| Product | HCID 58999582 | HCID 58999582 | — |
Reaction Steps
7-Benzyl-5,6,7,8-tetrahydro-[1,7]naphthyridin-4-ol (0.1 g, 0.417 mmol) in 3 ml of POCl3 was refluxed for 40 minutes. LCMS indicated complete coversion to the desired product. The excess POCl3 was removed under reduced pressure and taken on to the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07297700B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-fe67f152d4f64e04821378b9885cb05f |
| Source note | uspto-grants-2007_11 |